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49,80 €ISBN 978-3-8440-6733-0Softcover282 pages113 figures419 g21 x 14,8 cmEnglishThesis
June 2019
Daniel Haßkerl
Economic Performance Optimization by Direct Optimizing Control Applied to Reactive Distillation Processes
In diesem Werk wird die Anwendung der modellprädiktiven Echtzeit-Optimierung anhand eines Reaktivrektifikationsprozesses untersucht. Die Arbeit umreißt die Theorie der Zustandsschätzung und der Echtzeit-Optimierung anhand von ökonomischen Zielen und zeigt die Anforderungen an die mathematischen Formulierung und die Software-Realisierung auf. Das Werk beschäftigt sich im Schwerpunkt mit der Anwendung optimierender Regelung auf einen komplexen chemischen Prozess, einer zweistufigen Umesterungsreaktion, die in einer Reaktivrektifikationskolonne abläuft. So werden die verwendete Pilotanlage und die Ergebnisse aus den experimentellen Untersuchungen detailliert beschrieben und aufgeführt.
In this work, the application of model-based optimizing control applied to reactive distillation processes is presented. The theory of state estimation and of optimizing control are covered and the requirements for the mathematical definition and software realization for such applications are discussed. The main part of the work is dedicated to the application of optimizing control to a complex chemical process, reactive distillation. The main case study was a two-step transesterification reaction realized in a reactive distillation column. For this process the details of the setup of the column hardware in pilot-plant scale are shown and the results of the many experiments are presented.
In this work, the application of model-based optimizing control applied to reactive distillation processes is presented. The theory of state estimation and of optimizing control are covered and the requirements for the mathematical definition and software realization for such applications are discussed. The main part of the work is dedicated to the application of optimizing control to a complex chemical process, reactive distillation. The main case study was a two-step transesterification reaction realized in a reactive distillation column. For this process the details of the setup of the column hardware in pilot-plant scale are shown and the results of the many experiments are presented.
Keywords: Reactive Distillation; Model Predictive Control; Advanced Process Control
Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung
Edited by Prof. Dr.-Ing. Sebastian Engell, Dortmund
Volume 2019,2
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DOI 10.2370/9783844067330
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